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Spectrofluorimetric Determination of Formaldehyde in Maple Syrup

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A quick and simple method was developed for determination of formaldehyde in maple syrup. In this method, formaldehyde reacts with Fluoral P to form a complex which is chemically extracted by isobutanol and determined by spectrofluorimetry. Performance, as gauged by the limits of detection (0.16 mg/kg) and quantitation (0.21 mg/kg), recovery (>79%), and variability (1.9–16.1%, depending on fortification level and class of syrup) were superior to the current official AOAC standard method.
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Document Type: Research Article

Affiliations: 1: Centre ACER, Centre de Recherche, de Développement et de Transfert Technologique Acéricole, Inc., 3600 Casavant Blvd West, Saint-Hyacinthe, Québec, Canada J2S 8E3. 2: Canadian Food Inspection Agency, Ottawa Laboratory (Carling), Bldg 22, Ottawa, Ontario, Canada K1A 0C6. 3: Ministére de l'Agriculture, des Pêcheries et de l'Alimentation du Québec, Direction des Laboratoires d'Expertises et d'Analyses Alimentaires, 2700 Einstein, Sainte-Foy, Québec, Canada G1P 3W8.

Publication date: 2002-09-01

More about this publication?
  • The Journal of AOAC INTERNATIONAL publishes refereed papers and reviews in the fields of chemical, biological and toxicological analytical chemistry for the purpose of showcasing the most precise, accurate and sensitive methods for analysis of foods, food additives, supplements and contaminants, cosmetics, drugs, toxins, hazardous substances, pesticides, feeds, fertilizers and the environment available at that point in time. The scope of the Journal includes unpublished original research describing new analytical methods, techniques and applications; improved approaches to sampling, both in the field and the laboratory; better methods of preparing samples for analysis; collaborative studies substantiating the performance of a given method; statistical techniques for evaluating data. The Journal will also publish other articles of general interest to its audience, e.g., technical communications; cautionary notes; comments on techniques, apparatus, and reagents.
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